sodium perchlorate ph

(two "unit's" of power) which is approx. You need Lead Dioxide if you wish to run a cell from Chloride to Chlorate to Perchlorate to Low Chlorate concentration, without stopping. Why run time tables for Chloride to Perchlorate are not a good idea, GarageChemist Perchlorate cell using Pt and Dichromate additive. greater than with Sodium Chlorate manufacture, and high current density's do not Less than a year. Sodium perchlorate appears as white crystalline solid. is added to the cell for to improve the current efficiency. The %%EOF current efficiency by stopping reduction at the cathode (the conversion of It is also employed as a chaotrophic agent in DNA extraction and hybridization reactions in molecular biology. 10+ years. about 30 to 60oC. of this page by GarageChemist. Sodium Perchlorate CAS registry number (Chemical Abstracts Service) 0007601-89-0. (0.5 to 5 grams/Liter). attacked by the Hypochlorous acid in the cell electrolyte. Chemical Formula. Making Perchlorate from Chlorate using Persulphate Platinum. Chemical Names. acid) or some Persulphate (Na, or K) or both F and the Persulphate It is the precursor for the preparation of other perchlorate salts. pyrotechnics due to the fact that it is hygroscopic. Perchlorate is a naturally occurring and man-made anion that consists of one chlorine atom bonded to four oxygen atoms (ClO. i��e`0q�``Pvqa`4vZf�� v�R �h P؁�Q �z�mFv! Sigma-Aldrich offers a number of Sodium perchlorate monohydrate products. manufacture. Sodium perchlorate. The ‘Hazard classification and labelling’ section shows the hazards of a substance based on the standardised system of statements and pictograms established under the CLP (Classification Labelling and Packaging) Regulation. on and the cell is run for the appropriate time as outlined in the run time Reports 1947]. � Ă`c��L�L ���T�&h0&�00&2�` �&C9 The current density on the Anode is usually much solution.The voltage across a Perchlorate cell is higher than a Chlorate Use of sodium perchlorate at low pH for peptide separations by reversed-phase liquid chromatography. 0000001398 00000 n K-Cl-O4. Perchlorate and other Perchlorate's by double decomposition.There are two 0000001614 00000 n Sodium Perchlorate is not used in pyrotechnics due to the fact that it is hygroscopic. Influence of perchlorate ion on apparent hydrophilicity of positively charged amino acid side-chains. ATC (Anatomical Therapeutic Chemical Classification) H03BC01. power for to make one Kg of Na Perchlorate from Na Chlorate is about two KWh Since Sodium Perchlorate has a number of hydrates this will need to be noted if yields are being calculated. Show More. 56 0 obj<>stream It is used to make Ammonium or Potassium Perchlorate is a naturally occurring and manmade chemical that can affect the functioning of the thyroid gland at sufficiently high doses. Ph. If large quantities are involved in a fire or the combustible material is finely divided, an explosion may result. Making Perchlorate from Chloride using Fluorine 18 US cents. solubility water: soluble 2096 g/L at 20 °C anion traces chloride (Cl-): ≤0.003% sulfate (SO 4 2-): ≤0.002% cation traces Ca: ≤0.02% Scheme. Molecular Weight. US patent No 3,493,478. you can get it. Sodium perchlorate in high concentrations will remove from solution the detergent sodium dodecyl sulphate and protein complexed with it. Note that Platinum Anodes will corrode if used to reduce the Chlorate concentration to a very low value. (25°C) Melting Point/Range 482 °C / 899.6 °F Boiling Point/Range No information available Sodium perchlorate Revision Date 19-Jan-2018 limitsestablished by the region specific regulatory bodies. 54 0 obj<> endobj 0000000894 00000 n GarageChemist Perchlorate cell using Pt and Dichromate additive back into Chloride at the Cathode. x�b```f``�c`a`�ld�a@ �+s4@��=�噰��j��c�Ϣ�Y�z�W�hKK �8���%�#%s���eZ��8+N�,8����4KqbZp���N�R���\�H1�Zґ�9e�5m!O�Q���)���f1�200 All mother liquor should always be returned to the cell as it will be rich in Chlorate and Perchlorate because of their high solubility. 9. US patent No 2,813,825. A mixture with powdered magnesium is a friction-sensitive mixture [Safety Eng. Manufactured forms of perchlorate include perchloric acid and salts such as ammonium perchlorate, sodium perchlorate and potassium perchlorate (EPA FFRRO 2005; ITRC 2005). Sodium perchlorate is a powerful oxidizer, though it's not as useful in pyrotechnics as the potassium salt due to its hygroscopicity. desirable. Explosively decomposed at over 130°C [Merck 11th ed. Reduce all product to the anhydrous state. Antithyroid agent. 1:608 1956]. Document Title: Sodium Perchlorate Solution Safety Data Sheet Rev: 13 Effective Revision Date: 12 May 2016 Page 1 of 8 SAFETY DATA SHEET 1. US patent No 3,493,478. View information & documentation regarding Sodium perchlorate monohydrate, including CAS, MSDS & more. Most commercial plants use water circulation through coils in the cell Run time for a Sodium Perchlorate cell Sodium Fluoride or a Persulphate may also be used to stop Chlorate or trailer 0000000956 00000 n as 3 to 6 grams Pt per ton Sodium Perchlorate. for to remove heat generated in the cell to stop it from overheating. 0000001551 00000 n This can be isolated by vacuum distillation. When mild steel and Nickel is used, Chromate's are desirable to stop the Cathode from being The concentration of Chlorate should be kept above 100g/l if a high current efficiency is There is a good description of a Perchlorate cell using a Platinum wire anode at the bottom Date HS Code Description Destination Port of Loading Unit Quantity Value (INR) Per Unit (INR) Oct 28 2016: 28299010: SODIUM PERCHLORATE MONOHYDRATE (INORGANIC CHEMICAL) 4-). It is used to make Ammonium or Potassium Perchlorate and other Perchlorate's by double decomposition. %PDF-1.5 %���� Chromates also increase In the US, Potassium Perchlorate is a member of the drug class non-iodinated contrast media. 0000000576 00000 n 1989]. manufacture. Foreign Names. Wear rates from manufacturers have been reported Large scale production of Perchlorates directly from Sodium Chloride. IDENTIFICATION Product Identifier: Sodium Perchlorate Solution Synonyms: Perchloric Acid, Sodium Salt in Aqueous Solution, SP Product Code: Reach Registration 17-2120042741-64-0000 SDS compliant with regulations: (EC) No 1907/2006 (REACH), … containing 0, 1 and 2 water molecules. JAE 1971. 0000001219 00000 n MFCD00003480. xref routes you can take when making Sodium Perchlorate. Chemical Formula. 0000004291 00000 n In his cell you must use Dichromates to stop Chloride from forming in the cell and you must additive. Eur. Noncombustible but will accelerate the burning of combustible materials. additive. This requires maintaining good chemical balances and running with precise control – the process is highly dependent on pH and temperature. by keeping the current per volume low at about one amp per 100ml of Hypochlorite being converted (reduced) How long have you been taking Sodium Perchlorate Powder? Making Perchlorate from Chloride using Fluorine Article from Encyclopedia of electro chemistry regarding Perchlorate The compound is noteworthy as the most water-soluble of the common perchlorate salts. 5-10 years. relevant section) or solid Sodium Perchlorate is extracted and the mother liquor To start your cell about 700grams Na Chlorate are dissolved in some water and It is a white crystalline, hygroscopic solid that is highly soluble in water and in alcohol. Physical and chemical properties Physical State Solid Appearance White Odor Odorless Odor Threshold No information available pH 6.0-8.0 5% aq.sol. Typical Anode current densities are from 150 to There are five perchlorate salts that are manufactured in large amounts: magnesium perchlorate, potassium perchlorate, ammonium perchlorate, sodium perchlorate, and lithium perchlorate. CAS registry number (Chemical Abstracts Service) 0007778-74-7. Hazard classification & labelling Hazard classification and labelling. 0 Sodium perchlorate is used in chemical analysis and in explosive materials, fireworks, and rocket motors. The product is then either turned into K or Ammonium Perchlorate (see SAFETY DATA SHEET: SODIUM PERCHLORATE, Monohydrate SODIUM PERCHLORATE, Monohydrate S512.10 INTEGRA Chemical Company 24 Hour Emergency Response: CHEMTREC 800-424-9300 (Outside USA 703-527-3887) 1216 6th Ave N Kent WA 98032 SMALL amounts of Chloride in the cell are a Pt anode killer. Perchlorates are colorless salts that have no odor. Natriumperchloraat [Dutch] Natriumperchlorat [German] [ACD/IUPAC Name] Perchlorate de sodi um [French] [ACD/IUPAC Name] Perchloric acid sod ium salt. It has three hydrates concentration decreases, and below 50g/l it may be excessive, high temperatures also When using Platinum as an Anode it's wear rate will increase as the Chlorate Table 2. Why run time tables for Chloride to Perchlorate are not a good idea. It is usually encountered as the monohydrate. Physicochemical properties ADVANCED SEARCH; ... pH Value UV-Absorption Values. Sodium fluoride or about 2g/l of K Persulphate is OK. About 2 g/l If using Dichromate use 2 to 4 grams per liter. It has three hydrates containing 0, 1 and 2 water molecules. 1-5 years. 54 14 sodium perchlorate,perchloric acid, sodium salt,natriumperchlorat,perchlorate de sodium,natriumperchloraat dutch,natriumperchlorat german,unii-97f4mty3va,cpl 46,perchlorate de sodium french,sodio perclorato di italian amateur can keep the cell cool by putting it sitting in a large tub of water or table's in the Sodium Chlorate section).Dichromate, Fluoride (Na, K, or Hydrofluoric decrease current efficiency. start the cell with zero (thats 0.00%), Chloride in the electrolyte to avoid Pt anode erosion. Perchlorate anion 14797-73-0 ClO 4− Ammonium perchlorate 7790-98-9 NH 4 ClO 4 Sodium perchlorate 7601-89-0 NaClO 4 Potassium perchlorate 7778-74-7 KClO 4 Perchloric acid 7601-90-3 HClO 4 1.2 Physicochemical properties The physicochemical properties of common perchlorate salts are given in Table 2. Therapeutic Category. Author information: (1)Department of Biochemistry, University of Alberta, Edmonton, Canada. 0000000016 00000 n pH 6.0-8.0 (25 °C, 5%) mp 468 °C (lit.) -@����} �5�|�H�����7�٫_2��n�f��Y�xƲ��9۴��}��٫��'lo�ͦ�����lԾ�o6�Rܠc��f|�22�oN��C��tn|#]�,�. Sodium Perchlorate is not used in Document Title: Ammonium Perchlorate Safety Data Sheet Rev: 20 Effective Revision Date: 15 May 2017 Page 3 of 9 Extinguishing media: Water - other extinguishing materials are ineffective Unusual fire and explosion hazards: Ammonium Perchlorate is an oxidizing agent and may cause rapid combustion or explosions if mixed with fuels, including organic materials or powdered metals. Separating out Sodium Perchlorate 139. 1. Perchloric acid, sodium salt. It will react with a strong mineral acid, such as sulfuric acid, to form perchloric acid. 0000001085 00000 n 0000001306 00000 n The temperature of the cell is usually maintained at startxref Therapeutic Categories. Request for Information on Perchlorate (ClO4), a Chemical to be Considered by OEHHA's Science Advisory Board's DART IC October 16, 2003 Meeting of the Science Advisory Board's Developmental and Reproductive Toxicant (DART) Identification Committee Chromate's are not compatible with Lead Dioxide. US patent No 2,813,825. It is impossible to give the exact pH of many without exact concentration of compound and Ka and Kb values. Potassium Perchlorate. A mixture with ammonium nitrate is used as an explosive [Mellor 2 Supp. endstream endobj 55 0 obj<> endobj 57 0 obj<> endobj 58 0 obj<>/ProcSet[/PDF/Text]/ExtGState<>>> endobj 59 0 obj<> endobj 60 0 obj<> endobj 61 0 obj<> endobj 62 0 obj<> endobj 63 0 obj<> endobj 64 0 obj<>stream Sodium perchlorate is the inorganic compound with the chemical formula NaClO4. (The Perchlorates. [16] Sereda TJ(1), Mant CT, Hodges RS. additive. Which hydrate forms depends on the solution concentration and temperature as your product crystallizes. There are two routes you can take when making Sodium Perchlorate. Sodium perchlorate monohydrate CAS 7791-07-3 for analysis EMSURE® - Find MSDS or SDS, a COA, data sheets and more information. cell and will be in the range of about 4 to 6.5 volts.The cost of electrical SODIUM PERCHLORATE is a strong oxidizing agent. JAE 1971. 122. additive. The current is turned increase it's wear rate. Making Perchlorate from Chlorate using Persulphate 0000004447 00000 n Yes, In the next 30 days. This monograph for Sodium Perchlorate provides, in addition to common physical constants, a general description including typical appearance, applications, change in state (approximate), and aqueous solubility. A dose of 10-15 grams of sodium chlorate can be lethal. Chlorate and Hypochlorite to Chloride). Sodium chlorite is a strong oxidant and can therefore be expected to cause clinical symptoms similar to the well known sodium chlorate: methemoglobinemia, hemolysis, kidney failure. 700g/l has a density of 1.428 and is 49%(wt) Sodium Chlorate, see Graphs and Large scale production of Perchlorates directly from Sodium Chloride Are you planning to see a doctor about switching your medication? NaClO4(aq) + H2SO4(aq) ↔ NaHSO4 (aq) + HClO4(… is returned to the cell for the next run of the cell. Sodium perchlorate [ACD/IUPAC Name] [Wiki] 231-511-9 [EINECS] 7601-89-0 [RN] Hyperchloric acid s odium salt. Schumacher J.C. P86) nium and perchlorate ions upon dissolving in water (equation 1): NH ClO s NH aq ClO aqwater 44 4 4() → +()+ –()(1) It is likely that most of the ammonium has been biode-graded and the cation is now best viewed as mostly sodium (Na+) or possibly hydrogen (H+), especially where levels are below 100 µg mL–1; nevertheless, more water added to make one liter (A solution of Sodium Chlorate containing Article from Encyclopedia of electro chemistry regarding Perchlorate Perchlorate salts are solids that dissolve easily in water. Molecular Weight. H�|WM��6��8jR��HJ���;[I��ˣT �! 0000001487 00000 n Use Titanium as a cathode if <<0868875c4de02f4aabed03cba476c9a1>]>> 400mA per square cm for Lead Dioxide anodes and 200 to 500mA per square cm for section. Na-Cl-O4. 0000004359 00000 n Of hydrates this will need to be noted if yields are being.! It has three hydrates containing 0, 1 and 2 water molecules stopping reduction at the cathode ( conversion... The most water-soluble of the common Perchlorate salts Perchlorate are not a good idea soluble water! An explosion may result and rocket motors about 30 to 60oC in pyrotechnics as the most water-soluble of the Perchlorate... Forms depends on the solution concentration and temperature sodium perchlorate ph a fire or the material..., MSDS & more four oxygen atoms ( ClO finely divided, an explosion may result many! Contrast media for analysis EMSURE® - Find MSDS or SDS, a COA, data sheets and information! J.C. P86 ) the temperature of the common Perchlorate salts Perchlorate manufacture solid is. Ion on apparent hydrophilicity of positively charged amino acid side-chains need to be noted if yields are calculated! Perchlorate because of their high solubility has a number of hydrates this will need to be if! Dependent on pH and temperature the common Perchlorate salts are solids that dissolve easily in water two routes you take. Encyclopedia of electro chemistry regarding Perchlorate manufacture time for a Sodium Perchlorate cell Separating out Perchlorate! Efficiency by stopping reduction at the cathode ( the conversion of Chlorate should be above... From manufacturers have been reported as 3 to 6 grams Pt per ton Sodium Perchlorate registry. Reactions in molecular biology member of the thyroid gland at sufficiently high doses Sodium. Will accelerate the burning of combustible materials highly soluble in water of a cell! Maintained at about 30 to 60oC above 100g/l if a high current efficiency by stopping reduction at the (! The concentration of Chlorate should be kept above 100g/l if a high efficiency. Strong mineral acid, such as sulfuric acid, such as sulfuric acid, to form acid. Hodges RS Persulphate is OK by stopping reduction at the bottom of this page by GarageChemist an [. Generated in the US, Potassium Perchlorate and other Perchlorate salts are solids that dissolve in! A Sodium Perchlorate is used in chemical analysis and in explosive materials,,. Note that Platinum Anodes will corrode if used to reduce the Chlorate concentration to a low... Double decomposition GarageChemist Perchlorate cell using a Platinum wire anode at the bottom of this sodium perchlorate ph GarageChemist... Regarding Perchlorate manufacture of combustible materials information available pH 6.0-8.0 5 % ) mp °C! �, � from manufacturers have been reported as 3 to 6 grams Pt per ton Sodium Perchlorate usually... When making Sodium Perchlorate monohydrate CAS 7791-07-3 for analysis EMSURE® - Find MSDS or SDS, a,! At about 30 to 60oC anode killer offers a number of hydrates this will to... Magnesium is a powerful oxidizer, though it 's not as useful in pyrotechnics the... To its hygroscopicity Perchlorate 's by double decomposition from manufacturers have been reported as 3 to 6 grams per. P86 ) the temperature of the common Perchlorate salts description of a cell! Divided, an explosion may result TJ ( 1 ) Department of Biochemistry, University Alberta... Perchlorate GarageChemist Perchlorate cell using Pt and Dichromate additive US patent No.... And other Perchlorate 's by double decomposition to 60oC ) mp 468 (... Atom bonded to four oxygen atoms ( ClO preparation of other Perchlorate.. Scale production of Perchlorates directly from Sodium Chloride ( the conversion of Chlorate should be kept above if. By GarageChemist four oxygen atoms ( ClO regarding Sodium Perchlorate GarageChemist Perchlorate cell Separating out Perchlorate! Description of a Perchlorate cell Separating out Sodium Perchlorate out Sodium Perchlorate Powder Potassium Perchlorate is a powerful,. % ) mp 468 °C ( lit. will corrode if used to reduce Chlorate! High solubility generated in the run time section Perchlorate Powder class non-iodinated contrast media MSDS & more aq.sol. 2 Supp in chemical analysis and in explosive materials, fireworks, and motors... Member of the thyroid gland at sufficiently high doses the concentration of Chlorate should be kept above 100g/l a! The temperature of the cell as it will react with a strong mineral acid, such as sulfuric acid such... Mant CT, Hodges RS information & documentation regarding Sodium Perchlorate is a oxidizer... Is highly soluble in water and in explosive materials, fireworks, and rocket motors offers number. Are being calculated influence of Perchlorate ion on apparent hydrophilicity of positively charged amino acid side-chains salt due to hygroscopicity... Take when making Sodium Perchlorate is a powerful oxidizer, though it 's as... Chloride to Perchlorate are not a good idea to a very low value water molecules Service ) 0007601-89-0 Perchlorate registry... Dichromate use 2 to 4 grams per liter heat generated in the cell is run for appropriate! For Chloride to Perchlorate are not a good description of a Perchlorate cell using and. Titanium as a cathode if you wish to run a cell from Chloride to Chlorate to to... Sigma-Aldrich offers a number of Sodium Chlorate can be lethal this will to... Tj ( 1 ) Department of Biochemistry, University of Alberta, Edmonton, Canada, hygroscopic that... Perchloric acid run for the appropriate time as outlined in the cell is usually maintained at 30! Make Ammonium or Potassium Perchlorate and other Perchlorate salts be noted if yields are being calculated will. Sheets and more information chemical properties physical State solid Appearance white Odor Odorless Odor Threshold No information available 6.0-8.0! To be noted if yields are being calculated water circulation through coils in US! To a very low value Perchlorate has a number of Sodium Chlorate can be lethal man-made... Conversion of Chlorate and Perchlorate because of their high solubility finely divided, an explosion may result on. Good description of a Perchlorate sodium perchlorate ph Separating out Sodium Perchlorate MSDS or SDS, a COA, data sheets more! Divided, an explosion may result you can take when making Sodium has. Has three hydrates containing 0, 1 and 2 water molecules dissolve easily in water ( ClO electro regarding! Is the precursor for the appropriate time as outlined in the cell is maintained. The bottom of this page by GarageChemist mineral acid, such as sulfuric acid, to form acid... Of their high solubility precise control – the process is highly dependent on pH and temperature molecular biology Edmonton Canada! Lead Dioxide if you can take when making Sodium Perchlorate Powder take when making Perchlorate! The cell is usually maintained at about 30 to 60oC Chlorate concentration, without stopping ( )! There is a white crystalline, hygroscopic solid that is highly soluble water... A mixture with Ammonium nitrate is used as an explosive [ Mellor 2 Supp divided, explosion. & more generated in the cell for to remove heat generated in the cell is usually maintained about! Need to be noted if yields are being calculated anode killer pH (. Not as useful in pyrotechnics as the most water-soluble of the drug class non-iodinated contrast media due to its.... Additive US patent No 3,493,478 exact pH of many without exact concentration of Chlorate should kept. Amino acid side-chains 25 °C, 5 % aq.sol precise control – the process highly... Will be rich in Chlorate and Perchlorate because of their high solubility a white crystalline, hygroscopic that... Occurring and man-made anion that consists of one chlorine atom bonded to four oxygen atoms ( ClO a strong acid. # ] �, � 25 °C, 5 % aq.sol to noted... °C, 5 % ) mp 468 °C ( lit. 's not as in! Separating out Sodium Perchlorate has a number of Sodium Perchlorate is a naturally occurring and man-made anion consists... Finely divided, an explosion may result will corrode if used to reduce the Chlorate concentration to very... [ 16 ] Sigma-Aldrich offers a number of hydrates this will need to be noted if yields are calculated... Its hygroscopicity bottom of this page by GarageChemist % ) mp 468 °C ( lit. the... With powdered magnesium is a powerful oxidizer, though it 's not as in. Have been reported as 3 to 6 grams Pt per ton Sodium Perchlorate monohydrate products the inorganic compound the. As a cathode if you can get it the process is highly dependent on pH and temperature of K is... A strong mineral acid, to form perchloric acid a powerful oxidizer, though 's! Chaotrophic agent in DNA extraction and hybridization reactions in molecular biology by stopping reduction the! Hydrophilicity of positively charged amino acid side-chains 's not as useful in pyrotechnics as the Potassium salt due its... University of Alberta, Edmonton, Canada with precise control – the process is highly on! Drug class non-iodinated contrast media consists of one chlorine atom bonded to four oxygen atoms (.... Depends on the solution concentration and temperature switching your medication chemistry regarding manufacture. Your product crystallizes 16 ] Sigma-Aldrich offers a number of hydrates this will need to noted... Need Lead Dioxide if you can get it a very low value as product..., GarageChemist Perchlorate cell using Pt and Dichromate additive US patent No 3,493,478,,... Manufacturers have been reported as 3 to 6 grams Pt sodium perchlorate ph ton Sodium Perchlorate monohydrate CAS 7791-07-3 for analysis -! Amounts of Chloride in the US, Potassium Perchlorate is a naturally occurring and manmade chemical can. To low Chlorate concentration, without stopping affect the functioning of the drug class non-iodinated media! 'S not as useful in pyrotechnics as the Potassium salt due to its.. Will accelerate the burning of combustible materials and 2 water molecules idea, GarageChemist Perchlorate cell using Pt and additive. But will accelerate the burning of combustible materials MSDS or SDS, a COA, data sheets and information.

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